Réaction #1135813

Équation de réaction

1-ethoxy-2-methyl-3-nitrobenzene

→

3-ethoxy-2-methylaniline

Solvants

ethanol

Conditions de réaction

Traitement

1. 1
   FiltrationThe mixtures were filtered
2. 2
   Concentrationthe filtrates were concentrated

Mode opératoire

A mixture of 1-ethoxy-2-methyl-3-nitrobenzene described in Reference Preparation example 2539.9 g, palladium-carbon (palladium 5%) 4 g and ethanol 200 mL was stirred at room temperature under hydrogen atmosphere for eighteen hours. The mixtures were filtered and the filtrates were concentrated to give 3-ethoxy-2-methylaniline 33.0 g.

Source