Réaction #1106665

Équation de réaction

1,8-dichloroanthraquinone

N,N-dimethylethylenediamine

→

Compound 6

1,8-bis(2-(dimethylamino)ethylamino)anthracene-9,10-dione

Solvants

water

Conditions de réaction

Traitement

1. 1
   Températurewas refluxed for 18 h
2. 2
   Autreto precipitate the title compound which
3. 3
   Autrewas recrystallised from methanol

Mode opératoire

A mixture of 1,8-dichloroanthraquinone (5.5 g, 20 mmol) and N,N-dimethylethylenediamine (40 mL) was refluxed for 18 h. The mixture was cooled to room temperature and diluted with water to precipitate the title compound which was recrystallised from methanol to afford Compound 6 (4.5 g). The structure of Compound 6 is given below:

Source