Reacción #994
ord-d2aea31453084c8dba037f866c0833b5
Ecuación de reacción
2-Methoxy-cinnamylalcohol
thionylchloride
piperazine
→
salt
N,N'-bis-((E)-3-(2-methoxyphenyl)-2-propenyl)piperazine
Reactivos
Ninguno
Condiciones de reacción
Condiciones detalladas
See reaction.notes.procedure_details.
Tratamiento posterior
- 1Otroas described in Preparation Example 2
Procedimiento
2-Methoxy-cinnamylalcohol (1.44 g) was chlorinated using thionylchloride. Subsequently, reaction with piperazine and other treatments were performed as described in Preparation Example 2, to thereby obtain 314 mg of a salt as colorless prisms.