Reacción #992694

Ecuación de reacción

Glycolic acid

Guanidine carbonate

carbon dioxide

→

Guanidinium Glycolate

Disolventes

water

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThe water was removed in vacuo
2. 2
   Temperaturawith heating to approximately 90° C
3. 3
   OtroThe product was isolated as a white solid

Procedimiento

Glycolic acid (3.0 g, 39.45 mmol) was dissolved in 15 ml of distilled water. Guanidine carbonate (3.55 g, 19.72 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 4 hours. The water was removed in vacuo with heating to approximately 90° C. The product was isolated as a white solid.

Fuente