Reacción #992687

Ecuación de reacción

Tetrafluorosuccinic acid

Guanidine carbonate

carbon dioxide

→

Bis(guanidinium) Tetrafluorosuccinate

Disolventes

water

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThe water was removed in vacuo
2. 2
   Temperaturawith heating to approximately 90° C. for 4 hours
3. 3
   OtroThe product was isolated as a white solid

Procedimiento

Tetrafluorosuccinic acid (500 mg, 2.63 mmol) was dissolved in 10 ml of distilled water. Guanidine carbonate (474 mg, 2.63 mmol) was added at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 2 hours. The water was removed in vacuo with heating to approximately 90° C. for 4 hours. The product was isolated as a white solid.

Fuente