Reacción #985245
ord-2770af4c3d4f4844962ba4d053214fb5
Ecuación de reacción
Condiciones de reacción
Condiciones detalladas
See reaction.notes.procedure_details.
Tratamiento posterior
- 1workup.ADDITIONto mixing
- 2OtroThe initial solid phase formed immediately
- 3workup.ADDITIONon mixing
- 4Filtraciónwas filtered
- 5Lavadowashed (with distilled water+NaOH, pH 10)
- 6Otrofreeze-dried
Procedimiento
The calcium solution was added rapidly with stirring to the phosphate solution. All solutions were adjusted to pH 10 with concentrated NaOH prior to mixing. The initial solid phase formed immediately on mixing was filtered, washed (with distilled water+NaOH, pH 10), and then freeze-dried.