Reacción #985245

ord-2770af4c3d4f4844962ba4d053214fb5

Ecuación de reacción

Reactivos

Ninguno

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    workup.ADDITIONto mixing
  2. 2
    OtroThe initial solid phase formed immediately
  3. 3
    workup.ADDITIONon mixing
  4. 4
    Filtraciónwas filtered
  5. 5
    Lavadowashed (with distilled water+NaOH, pH 10)
  6. 6
    Otrofreeze-dried

Procedimiento

The calcium solution was added rapidly with stirring to the phosphate solution. All solutions were adjusted to pH 10 with concentrated NaOH prior to mixing. The initial solid phase formed immediately on mixing was filtered, washed (with distilled water+NaOH, pH 10), and then freeze-dried.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07351280B2uspto-grants-2008_04