Reacción #955933

Ecuación de reacción

methyl 2,4-dimethylbenzoate

hydrazine

→

2,4-dimethylbenzohydrazide

Disolventes

MeOH

Condiciones de reacción

Tratamiento posterior

1. 1
   Temperaturathe mixture was heated
2. 2
   Temperaturaunder reflux for 40 hours
3. 3
   OtroThen the mixture was evaporated
4. 4
   Otrodried under vacuum

Procedimiento

To a solution of methyl 2,4-dimethylbenzoate (2 g, 12.2 mmol) in MeOH (10 mL) was added anhydrous hydrazine (1.95 mL, 61 mmol) and the mixture was heated under reflux for 40 hours. Then the mixture was evaporated and dried under vacuum to give 2,4-dimethylbenzohydrazide as a white solid (2 g, 100%; MS (M+H, 165).

Fuente