Reacción #94287

ord-52353e447c8043f5952fcb5206d578ee

Ecuación de reacción

Clc1ccc(CN2CCNCC2)cc1
1-p-chlorobenzyl-piperazine
CCOC(=O)c1cn(CC)c2nc(Cl)ncc2c1=O
2-chloro-5-oxo-6-carbethoxy-8-ethyl-5,8-dihydro-pyrido(2,3-d)pyrimidine
CCOC(=O)c1cn(CC)c2nc(N3CCN(Cc4ccc(Cl)cc4)CC3)ncc2c1=O
2-(4'-p-chlorobenzyl-piperazino)-5-oxo-6-carbethoxy-8-ethyl-5,8-dihydro-pyrido(2,3-d)pyrimidine
Rendimiento 74.0%

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

Condensation of 1-p-chlorobenzyl-piperazine with 2-chloro-5-oxo-6-carbethoxy-8-ethyl-5,8-dihydro-pyrido(2,3-d)pyrimidine, as described in Example VII, gives, in a yield of 74%, 2-(4'-p-chlorobenzyl-piperazino)-5-oxo-6-carbethoxy-8-ethyl-5,8-dihydro-pyrido(2,3-d)pyrimidine; melting point 150° C., after recrystallisation from ethyl acetate.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US04129737uspto-grants-1978_12