Reacción #94108

Ecuación de reacción

salicylaldehyde

1,12-diaminododecane

→

N,N'-Bis-(2-hydroxybenzyl)-dodecamethylenediamine

Disolventes

isopropanol

Condiciones de reacción

Procedimiento

30.0 g of a bisazomethine prepared from 2 mols of salicylaldehyde and 1 mol of 1,12-diaminododecane and having a melting point of 72°-73° C. are hydrogenated for 2 hours in 300 ml of isopropanol in an autoclave in the presence of 3 g of Raney nickel at 90°-100° C. and under a pressure of 60 atmospheres

Fuente