Reacción #9346

Ecuación de reacción

Sodium propanoate

2,6-dipropylphenol

→

phenol

2,6-dipropyl-4-propionylphenol

Disolventes

Triflic Acid

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThe resulting waxy solid was purified by chromatography on silica gel

Procedimiento

Sodium propanoate (0.88 g, 1.5 eq) and 2,6-dipropylphenol (1.09 g, 1.0 eq) were combined in Triflic Acid (5.0 g) as in Example 13, step 1. The resulting waxy solid was purified by chromatography on silica gel using ethyl acetate:hexanes:acetic acid (10:90:1) to give the titled phenol.

Fuente