Reacción #927676

Ecuación de reacción

cyclopentadiene

tetrahydrofuran

2-hydroxyethyl acrylate

→

title compound

Rendimiento 85.0%

2-hydroxyethyl-5-norbornene-2-carboxylate

Rendimiento 85.0%

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThe solvent was removed by distillation through a rotary distiller

Procedimiento

About 66 g of cyclopentadiene is dissolved in about 500 g of tetrahydrofuran (THF). To the resulting mixture was added 130 g of 2-hydroxyethyl acrylate, and the reaction mixture was stirred at −30° C. for 10 hours. The solvent was removed by distillation through a rotary distiller. The title compound was obtained by distillation under reduced pressure (yield: 85%).

Fuente