Reacción #92544

ord-9d3ab2e2655f49399e011c7ac61de0ce

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

The desired product was prepared from 4-(benzyloxy)benzoic acid according to the procedures similar to those (step 1 to 3) for 5-amino-3-(4-phenoxyphenyl)-1H-pyrazole-4-carbonitrile under appropriate conditions recognized by one of ordinary skill in the art. 1H NMR (400 MHz, DMSO-d6) δ 12.01 (s, 1H), 7.72 (d, J=8.8 Hz, 2H), 7.50-7.44 (m, 2H), 7.44-7.37 (m, 2H), 7.36-7.32 (m, 1H), 7.11 (d, J=7.2 Hz, 2H), 6.39 (br s, 2H) and 5.16 (s, 2H).

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US09447106B2uspto-grants-2016_09