Reacción #87648

ord-e69c6750c6694d3c9d9b32d018d9e3df

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    OtroThe title compound was prepared

Procedimiento

The title compound was prepared according to the procedure described in step-2 of Intermediate-26 by using 5-((2,2,2-trifluoroacetamido)methyl)-2-chloro-4-methoxybenzoic acid (1.0 g), oxalyl chloride (1.0 mL), THF (50 mL) and ammonia gas to afford 0.800 g of the desired product.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US09439890B2uspto-grants-2016_09