Reacción #83757

Ecuación de reacción

methyl 7-azaindol-1-acetate

lithium aluminum hydride

→

title compound

Rendimiento 87.1%

2-(7-Azaindol-1-yl)ethanol

Rendimiento 87.1%

Disolventes

tetrahydrofuran

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroA procedure similar to that described in Preparation 2

Procedimiento

A procedure similar to that described in Preparation 2 was repeated, except that 7.50 g of methyl 7-azaindol-1-acetate (prepared as described in Preparation 17), 1.80 g of lithium aluminum hydride and 260 ml of anhydrous tetrahydrofuran were used, to give 5.57 g of the title compound, melting at 52.7°-53.3° C.

Fuente