Reacción #83371

Ecuación de reacción

2-(4-Aminophenylthio)quinoline

3,4-dichlorophenylisothiocyanate

→

title compound

1-[4-(2-Quinolylthio)phenyl]-3-(3,4-dichlorophenyl)thiourea

Condiciones de reacción

Procedimiento

2-(4-Aminophenylthio)quinoline (11.9 moles, 3.0 g) and 3,4-dichlorophenylisothiocyanate (11.9 mmoles, 2.42 g) were reacted according to procedure B to yield the title compound, 360 mg, 6.6%. Mass Spec (FD) 455. Calculated for C22H15Cl2N3S2 : C, 57.90 H, 3.31; N, 9.21. Found: C, 57.86; H, 3.53; N, 9.07. m.p. 125°-126°.

Fuente