Reacción #833510

Ecuación de reacción

Vanillin

allyl bromide

potassium carbonate

→

3-methoxy-4-(2-propenyloxy)benzaldehyde

Disolventes

acetone

Condiciones de reacción

Tratamiento posterior

1. 1
   TemperaturaAfter cooling
2. 2
   Filtraciónthe solid was filtered off
3. 3
   Lavadowashed with acetone
4. 4
   OtroA yellow oil was obtained
5. 5
   Concentraciónafter a thorough concentration of the organic phases

Procedimiento

Vanillin (20.0 g, 0.130 mol) and allyl bromide (19.9 g, 0.160 mol) were heated under reflux together with potassium carbonate (27.3 g, 0.200 mol) in 150 ml acetone (abs.) for 8 hours. After cooling, the solid was filtered off and washed with acetone. A yellow oil was obtained after a thorough concentration of the organic phases.

Fuente