Reacción #82144

ord-165c21acb8a34d9c9681683a969f54e5

Ecuación de reacción

Reactantes

Reactivos

Ninguno

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    FiltraciónThe polymer was filtered
  2. 2
    ExtracciónThe ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor
  3. 3
    Otrodried
  4. 4
    Otroto afford a pale brown solid which

Procedimiento

The resulting heterogeneous reaction mixture, which was lumpy and hardened, was neutralized by addition of 15% aqueous tartaric acid solution. The polymer was filtered and a small portion was ground thoroughly. The ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor and dried to afford a pale brown solid which was not soluble to any extent in distilled water.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US05621088uspto-grants-1997_04