Reacción #82144
ord-165c21acb8a34d9c9681683a969f54e5
Ecuación de reacción
Reactantes
Reactivos
Ninguno
Disolventes
Condiciones de reacción
Condiciones detalladas
See reaction.notes.procedure_details.
Tratamiento posterior
- 1FiltraciónThe polymer was filtered
- 2ExtracciónThe ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor
- 3Otrodried
- 4Otroto afford a pale brown solid which
Procedimiento
The resulting heterogeneous reaction mixture, which was lumpy and hardened, was neutralized by addition of 15% aqueous tartaric acid solution. The polymer was filtered and a small portion was ground thoroughly. The ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor and dried to afford a pale brown solid which was not soluble to any extent in distilled water.