Reacción #816360

ord-96ee767b03f14d23acb1cdfa44e1e8db

Ecuación de reacción

CCN1CCCC1(C)C(Cl)(CC)CC
2-(1-chloro-1-ethylpropyl)methyl-1-ethylpyrrolidine
CNC
dimethylamine
CCN1CCCC(N(C)C)C1(CC)CC
3-dimethylamino-1,2,2-triethylpiperidine

Disolventes

Condiciones de reacción

Temperatura
40°CELSIUS
Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

A four-necked pear-shaped flask (500 mL) was charged with 14.04 g (0.07 mol) of 2-(1-chloro-1-ethylpropyl)methyl-1-ethylpyrrolidine, 54.26 g (0.48 mol) of a 40% aqueous dimethylamine solution, and 100 mL of ethanol, and the mixture was stirred at 40° C. for 44 hours.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07582124B2uspto-grants-2009_09