Reacción #7552

Ecuación de reacción

carbonate

oxalic acid

→

carbonate oxalate

Disolventes

ethyl acetate

ethyl acetate

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThe crystals precipitated
2. 2
   Filtraciónwere collected by filtration

Procedimiento

In 7 mL of ethyl acetate was dissolved 0.31 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=methyl=carbonate, and to the solution was added a solution of 0.10 g of oxalic acid in 1 mL of ethyl acetate, after which the resulting mixture was stirred at room temperature. The crystals precipitated were collected by filtration to obtain 0.34 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=methyl=carbonate oxalate.

Fuente