Reacción #74686

Ecuación de reacción

triphenylphosphine

chloromethyl ethyl ether

→

(Ethoxymethyl)triphenylphosphonium chloride

Disolventes

benzene

Condiciones de reacción

Tratamiento posterior

1. 1
   TemperaturaThe mixture then was chilled
2. 2
   Filtraciónfiltered
3. 3
   Otroto give 7

Procedimiento

A solution of 99.66 g of triphenylphosphine and 37.82 g of chloromethyl ethyl ether in 240 ml of dry benzene was stirred and refluxed (84° C.) for 6 hours. The mixture then was chilled and filtered to give 7, as a white solid, mp 205°-206° C.

Fuente