Reacción #730461

ord-da364bd7ed204dd4bf273626c15fda0b

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    OtroThe crystalline product was recrystallized from ethanol (96%)

Procedimiento

Methyl-6-bromo-2-naphtoate (25 g, 94.3 mmol) was reduced with lithiumaluminiumhydride (5.36 g, 141.4 mmol) in tetrahydrofuran (200 ml). The crystalline product was recrystallized from ethanol (96%). Yield 15.84 g (70.8%).

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07700596B2uspto-grants-2010_04