Reacción #71574

Ecuación de reacción

1,4-dithiane

tetrahydrofuran

methyltrifluoromethane sulfonate

→

Methyl-Dithiane Triflate

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroAfter 20 minutes a white solid product was obtained in a salt form
2. 2
   FiltraciónThe solid product was filtered
3. 3
   Otrodried for 1 hour in an oven at 50° C.
4. 4
   Otroto obtain the following product

Procedimiento

2 mmol of 1,4-dithiane was dissolved in 8 ml of tetrahydrofuran at 0° C., and about 2 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture. After 20 minutes a white solid product was obtained in a salt form. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:

Fuente