Reacción #71259

ord-a22ec2a4848845ee8dad873524be504d

Ecuación de reacción

CCCCCCCCCCCC(=O)OCC(O)CO
glycerol monolaurate
CCCCCCCCCCCCCCCCO
cetyl alcohol
CCCCCCCCCCCC(=O)OCC(O)CO
glycerol monolaurate
CCCCCCCCCCCCCCCCO
cetyl alcohol
CCCCCCCCCCCCCCCCCC(=O)O
stearic acid
CCCCCCCCCC[N+](C)(C)CCCCCCCCCC.[Cl-]
DDAC
→
CCCCCCCCCCCCCCCCCC(=O)O.OCCN(CCO)CCO
Triethanolamine Stearate

Reactantes

CCCCCCCCCCCC(=O)OCC(O)CO
glycerol monolaurate
CCCCCCCCCCCCCCCCO
cetyl alcohol
CCCCCCCCCCCC(=O)OCC(O)CO
glycerol monolaurate
CCCCCCCCCCCCCCCCO
cetyl alcohol
CCCCCCCCCCCCCCCCCC(=O)O
stearic acid
CCCCCCCCCC[N+](C)(C)CCCCCCCCCC.[Cl-]
DDAC

Reactivos

Ninguno

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    workup.ADDITIONInstead of being added in the second step
  2. 2
    workup.ADDITIONwas added
  3. 3
    workup.ADDITIONafter the addition of TEA

Procedimiento

Example 2A was repeated but for the sequence of addition of glycerol monolaurate and cetyl alcohol. Instead of being added in the second step, after the equimolar mixture of stearic acid and DDAC, the same amount of the glycerol monolaurate and cetyl alcohol added in Example 2 was added after the addition of TEA.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08536228B2uspto-grants-2013_09