Reacción #709528

Ecuación de reacción

2-amino benzoic acid hydrochloride

diphosgene

→

Isatoic anhydride

Disolventes

dioxane

Condiciones de reacción

Tratamiento posterior

1. 1
   Temperaturaat reflux
2. 2
   TemperaturaThe resulting mixture was cooled
3. 3
   Filtraciónfiltered

Procedimiento

7.5 g of 2-amino benzoic acid hydrochloride was mixed with 10 ml of diphosgene and the mixture was stirred in 150 ml of dioxane for 40 minutes at reflux. The resulting mixture was cooled and filtered. Yield: 5.7 g of title compound.

Fuente