Reacción #69567

Ecuación de reacción

2,2′-dimethyl-5,5′-bis(1-adamantyl)-biphenyl

2,2′-dimethyl-5,5′-bis(3-bromo-1-adamantyl)biphenyl

→

2,2′-dimethyl-5,5′-bis(3-(3,5-diethynylphenyl)-1-adamantyl)biphenyl

Rendimiento 73.5%

Condiciones de reacción

Tratamiento posterior

1. 1
   Otrothe same method as in Synthesis Example 3

Procedimiento

From the obtained 2,2′-dimethyl-5,5′-bis(1-adamantyl)-biphenyl 10 g, the same method as in Synthesis Example 7 was used to synthesize 2,2′-dimethyl-5,5′-bis(3-bromo-1-adamantyl)biphenyl 4.5 g, then the same method as in Synthesis Example 3 was used to obtain 2,2′-dimethyl-5,5′-bis(3-(3,5-diethynylphenyl)-1-adamantyl)biphenyl 3.8 g.

Fuente