Reacción #68859

Ecuación de reacción

6-chloro-2-methyl-quinoline

1,4-dioxane

→

title compound

6-Chloro-quinoline-2-carbaldehyde

Condiciones de reacción

Tratamiento posterior

1. 1
   FiltraciónThe resulting black mixture was filtered through diatomaceous earth

Procedimiento

A suspension of 6-chloro-2-methyl-quinoline (355 mg) and SeO2 (233 mg) in 1,4-dioxane (3 mL) was heated at 80° C. for 16 h. The resulting black mixture was filtered through diatomaceous earth. Concentration of the filtrate gave the title compound as a yellow powder (324 mg).

Fuente