Reacción #677124

Ecuación de reacción

Ammonium acetate

CH3CN

→

THF tetrahydrofuran

Condiciones de reacción

Tratamiento posterior

1. 1
   workup.WAITstaying at 95% B for 1.2 minute
2. 2
   OtroGeneral Procedure of Preparation

Procedimiento

Analytical HPLC/MS Analytical HPLC/MS was performed on a system consisting of a Waters Acquity UPLC, Waters Micromass LCT Premier XE mass spectrometer, Waters Acquity PDA. Column: Acquity UPLC HSS T3 1.8 μm; 2.1×50 mm; solventsystem: A=10 mM Ammonium acetate+0.1% HCOOH and B═CH3CN+0.1% HCOOH; flow rate=0.7 mL/min; method (4.8 min): Linear gradient method going from 1% B to 95% B in 2.6 minutes and staying at 95% B for 1.2 minute. General Procedure of Preparation:

Fuente