Reacción #669980

ord-04bb0291bcd64345a483338c57e0abaa

Ecuación de reacción

CCOC(CCO)OCC
3, 3-diethoxypropanol
[K].c1ccc2ccccc2c1
potassium naphthalene
[K]
potassium
CCOC(CCO)OCC
3, 3-diethoxypropanol

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

A reactor was charged with 30 ml of THF, 0.13 g of 3, 3-diethoxypropanol and 2 ml solution of potassium naphthalene dissolved in tetrahydrofuran in a concentration of 0.5 mol/L-tetrahydrofuran, and the resulting mixture was stirred for three minutes in an argon atmosphere, and, thus, there was formed a potassium derivative (potassium 3, 3-diethoxypropanoxide) of 3, 3-diethoxypropanol.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US05925720uspto-grants-1999_07