Reacción #6683

Ecuación de reacción

[R]-1-trifluoromethylheptyl 4-benzyloxybenzoate

→

[R]-1-Trifluoromethylheptyl 4-hydroxybenzoate

Rendimiento 99.0%

Disolventes

ethyl acetate

Condiciones de reacción

Tratamiento posterior

1. 1
   FiltraciónThen the catalyst was filtered out
2. 2
   Otrofiltrate was evaporated to dryness
3. 3
   Otroto give the pure compound in yield of 99%

Procedimiento

2.2 g of [R]-1-trifluoromethylheptyl 4-benzyloxybenzoate, (13) 100 mg of PdOH/C in 50 ml of ethyl acetate was stirred at RT over night under H2 atmosphere. Then the catalyst was filtered out and filtrate was evaporated to dryness to give the pure compound in yield of 99%.

Fuente