Reacción #66590

Ecuación de reacción

Iodomethane

3-((dimethylamino)methyl)-5-methylhexan-2-one

→

title product

Rendimiento 68.4%

(2-Acetyl-4-methyl-pentyl)-trimethyl-ammonium iodide

Rendimiento 68.4%

Disolventes

ethyl acetate

Condiciones de reacción

Tratamiento posterior

1. 1
   Filtración, and the resulting preciptant was collected by filtration

Procedimiento

Iodomethane (20 g, 140.94 mmol, 2.00 equiv) was added dropwise to a solution of 3-((dimethylamino)methyl)-5-methylhexan-2-one (12 g, 70.05 mmol, 1.00 equiv) and ethyl acetate (50 mL). The solution was stirred at ambient temperature for about 16 hours., and the resulting preciptant was collected by filtration to afford the title product (15 g, yield=68%).

Fuente