Reacción #66010

Ecuación de reacción

allyl bromide

diethylene glycol

→

Diethylene glycol monoallyl ether

Rendimiento 82.0%

Disolventes

THF NaH

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThe product was obtained in 82% yield
2. 2
   workup.DISTILLATIONafter distillation

Procedimiento

Diethylene glycol monoallyl ether was prepared by reacting allyl bromide with excess diethylene glycol in THF-NaH (tetrahydrofuran-sodium hydride). The product was obtained in 82% yield after distillation. b.p.=96-99° C./7 mmHg.

Fuente