Reacción #658770

Ecuación de reacción

9-phenylanthracene

bromosuccinimide

→

9-bromo-10-phenylanthracene

Rendimiento 89.3%

Disolventes

N,N dimethylformamide

Condiciones de reacción

Tratamiento posterior

1. 1
   Otroto react for six hours
2. 2
   workup.DISTILLATIONThen, distilled water
3. 3
   workup.ADDITIONwas added
4. 4
   Otrothe reaction
5. 5
   Filtraciónthe deposit was filtered
6. 6
   OtroThe recovered deposit was purified by column chromatography

Procedimiento

An amount of 13.65 (53.7 mmol) of 9-phenylanthracene was dissolved in 100 ml of N,N dimethylformamide. An amount of 10.5 g (59 mmol) of N bromosuccinimide was added and allowed to react for six hours. Then, distilled water was added to stop the reaction and the deposit was filtered. The recovered deposit was purified by column chromatography to obtain 15.97 g (48 mmol) of 9-bromo-10-phenylanthracene. The yield was 89.3%.

Fuente