Reacción #657025

ord-4d5dd1a7426248bba64714e0f0d4f721

Ecuación de reacción

C[C@@H](N)C(=O)O
D-alanine
CCCCCC(=O)Cl
hexanoyl chloride
CCCCCC(=O)N[C@H](C)C(=O)O
title compound
CCCCCC(=O)N[C@H](C)C(=O)O
(2R)-2-(Hexanoylamino)propionic acid

Reactivos

Ninguno

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

D-alanine (20 mmol) and hexanoyl chloride (22 mmol) were reacted using the method as described in Example 1 Part B to give the title compound as a white crystalline material (2.45 g, 65.5%) after recrystallization from isopropyl ether (20 ml), m.p. 82°-95° C.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US04734426uspto-grants-1988_03