Reacción #64598

Ecuación de reacción

n-butylmethylamine

N,N-dimethylacetamide dimethyl acetal

→

N-butyl-N-methylacetamide dimethyl acetal

Condiciones de reacción

Tratamiento posterior

1. 1
   workup.DISTILLATIONSubsequent vacuum distillation

Procedimiento

6.1 g (0.07 mol) of n-butylmethylamine are stirred with 9.3 g (0.07 mol) of N,N-dimethylacetamide dimethyl acetal for 24 hours under reflux at a bath temperature of 130° C. Subsequent vacuum distillation gives N-butyl-N-methylacetamide dimethyl acetal, bp 72°-75° C./31 mbar.

Fuente