Reacción #64223

Ecuación de reacción

acetone cyanohydrin

4-amino 1-butanol

→

propanonitrile

2-(4-hydroxybutylamino) 2-methylpropano-nitrile

Disolventes

methylene chloride

Condiciones de reacción

Tratamiento posterior

1. 1
   Otrodried
2. 2
   Filtraciónfiltered
3. 3
   Concentraciónthe filtrate was concentrated under reduced pressure

Procedimiento

220 μl of acetone cyanohydrin and 200 μl of 4-amino 1-butanol were mixed together with stirring for 16 hours at 20° C. and then was diluted with 2 ml of methylene chloride, dried, filtered and the filtrate was concentrated under reduced pressure to obtain the propanonitrile which was used as is for the following stage.

Fuente