Reacción #640553

Ecuación de reacción

Hexyltrimethylammonium hydroxide

tetraethylorthosilicate

→

Hexyltrimethylammonium Silicate

Disolventes

water

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroAfter hydrolysis
2. 2
   Otrothe solution was placed on a rotary evaporator
3. 3
   Otroto remove the alcohol
4. 4
   OtroA total of 518.6 g of liquid was removed
5. 5
   workup.ADDITIONafter which 150 g of deionized water was added

Procedimiento

Hexyltrimethylammonium hydroxide, (30.03%), 492.96 g, was diluted with 1073.86 g deionized water and to it there were added 650.0 g of tetraethylorthosilicate, (98%) with stirring. After hydrolysis was complete, the solution was placed on a rotary evaporator to remove the alcohol. A total of 518.6 g of liquid was removed, after which 150 g of deionized water was added. Elemental analysis showed the solution to contain 5.10 wt % Si.

Fuente