Reacción #63278

Ecuación de reacción

N-(1-phenyl-3-pyrrolidinopropyl)quinaldinamide

oxalic acid dihydrate

→

subject compound

Rendimiento 96.0%

N-(1-phenyl-3-pyrrolidinopropyl)quinaldinamide oxalate

Rendimiento 96.0%

Disolventes

ethanol

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThe resulting solution was evaporated under reduced pressure
2. 2
   Otroto remove the solvent
3. 3
   OtroThe residue was recrystallized from a mixture of acetone (6 ml) and diethyl ether (3 ml)

Procedimiento

In ethanol were dissolved 259 mg (0.72 mmol.) of N-(1-phenyl-3-pyrrolidinopropyl)quinaldinamide and 91 mg of oxalic acid dihydrate. The resulting solution was evaporated under reduced pressure to remove the solvent. The residue was recrystallized from a mixture of acetone (6 ml) and diethyl ether (3 ml) to obtain 310 mg (yield: 96%) of the subject compound as a white crystalline product.

Fuente