Reacción #632014
ord-65b08521242f4ac7b945aba117f89ee2
Ecuación de reacción
1-methoxymethylcyclopropylsulfonylamine tert-butyl-carbamate
n-propyl isocyanate
→
1-propylcarbamoylcyclopropanesulfonamide tert-butylcarbamate
Rendimiento 100.0%
Reactivos
Ninguno
Condiciones de reacción
Condiciones detalladas
See reaction.notes.procedure_details.
Tratamiento posterior
- 1OtroThis compound was obtained in a crude 100% yield
- 2OtroThe compound was taken directly into the next reaction without purification
Procedimiento
This compound was obtained in a crude 100% yield according to the procedure described for the synthesis of 1-methoxymethylcyclopropylsulfonylamine tert-butyl-carbamate using 1.10 equivalents of n-propyl isocyanate as the electrophile. The compound was taken directly into the next reaction without purification: 1H NMR (CDCl3) δ 0.10 (m, 2H), 0.51 (m, 2H), 0.67 (m, 1H), 1.10 (m, 2H), 1.49 (s, 9H), 1.62 (m, 2H), 1.87 (d, J=7.0 Hz, 2H).