Reacción #62847

ord-dda9c99e1c1445d2964589abf8008a1d

Ecuación de reacción

CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC(=O)O
3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid
CCN1CCCC1CN
2-aminomethyl-1-ethylpyrrolidine
→
CCN1CCCC1CNC(=O)C=C(C)CCC=C(C)CCC=C(C)CCC=C(C)C
title compound
Rendimiento 94.0%
CCN1CCCC1CNC(=O)C=C(C)CCC=C(C)CCC=C(C)CCC=C(C)C
2-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoylaminomethyl)-1-ethylpyrrolidine
Rendimiento 94.0%

Reactantes

CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC(=O)O
3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid
CCN1CCCC1CN
2-aminomethyl-1-ethylpyrrolidine

Reactivos

Ninguno

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

The procedure of Example 9 was repeated except that 6.1 g of 3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid and 3.8 g of 2-aminomethyl-1-ethylpyrrolidine were used as starting materials. 7.8 g (yield 94%) of the title compound was obtained as a brown oil.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US04762829uspto-grants-1988_08