Reacción #610117

Ecuación de reacción

1,8-dichloroanthraquinone

N,N-dimethylethylenediamine

→

Compound 6

1,8-bis(2-(dimethylamino)ethylamino)anthracene-9,10-dione

Disolventes

water

Condiciones de reacción

Tratamiento posterior

1. 1
   Temperaturawas refluxed for 18 h
2. 2
   Otroto precipitate the title compound which
3. 3
   Otrowas recrystallised from methanol

Procedimiento

A mixture of 1,8-dichloroanthraquinone (5.5 g, 20 mmol) and N,N-dimethylethylenediamine (40 mL) was refluxed for 18 h. The mixture was cooled to room temperature and diluted with water to precipitate the title compound which was recrystallised from methanol to afford Compound 6 (4.5 g). The structure of Compound 6 is given below:

Fuente