Reacción #59923

Ecuación de reacción

( 8b )

2-(2-propyl-1,3-dioxan-2-yl)ethanol

ethyl acetoacetate

2,2-dimethyl-1,3-propanediol

→

title compound

Rendimiento 55.0%

2-(2,5,5-trimethyl-1,3-dioxan-2-yl)ethanol

Rendimiento 55.0%

Condiciones de reacción

Procedimiento

The same procedure as in the steps (8a) and (8b) of Example 8 was repeated using ethyl acetoacetate, and 2,2-dimethyl-1,3-propanediol to obtain the title compound (7.3 g, total yield: 55%) as a light yellow oil.

Fuente