Reacción #58756

Ecuación de reacción

6-bromo-pyridine-2-carbaldehyde

2-methoxy-ethylamine

→

title compound

Rendimiento 94.0%

(6-Bromo-pyridin-2-ylmethyl)-(2-methoxy-ethyl)-amine

Rendimiento 94.0%

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThe title compound was prepared in a manner similar to
2. 2
   OtroThe crude product was purified (SiO2: 0-5% MeOH/DCM)

Procedimiento

The title compound was prepared in a manner similar to that described in Example 18, Step C, using 6-bromo-pyridine-2-carbaldehyde (0.275 g, 1.48 mmol) and 2-methoxy-ethylamine (0.111 g, 1.48 mmol). The crude product was purified (SiO2: 0-5% MeOH/DCM) to yield the title compound (0.34 g, 94%).

Fuente