Reacción #58312

Ecuación de reacción

2-bromo-5-methoxybenzoic acid

n-butyllithium

N-methoxy-N-methylnicotinamide

→

5-methoxy-2-pyridin-3-ylbenzoic acid

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThis compound is synthesized
2. 2
   OtroAfter precipitation in aqueous phase at pH 4
3. 3
   Filtraciónfollowed by filtration
4. 4
   Otrodrying
5. 5
   Otroa beige-coloured powder is obtained

Procedimiento

This compound is synthesized according to the method described in 3.2. by reacting 2-bromo-5-methoxybenzoic acid pretreated with n-butyllithium with N-methoxy-N-methylnicotinamide. After precipitation in aqueous phase at pH 4, followed by filtration and drying, a beige-coloured powder is obtained.

Fuente