Reacción #581970

ord-03a1b27308494746994172ea3409ec11

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

The product from Example 23D and isobutyl(methyl)amine were processed as described in Example 1D to provide the titled compound. 1H NMR (300 MHz, CD3OD) δ 7.82 (m, 1H), 7.74 (d, J=8.1, 2H), 7.58 (m, 2H), 7.51 (d, J=8.1 Hz, 2H), 6.81 (s, 1H), 3.3-3.8 (m, 14H), 2.96 (s, 3H), 2.2 (m, 1H), 1.09 (d, J=6.6 Hz, 6H); MS (DCI) m/z 421 (M+H)+;

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07538138B2uspto-grants-2009_05