Reacción #575884

ord-da50336a33da4c0bb3d2bf80e1481ee7

Ecuación de reacción

CNC1(C)C2CCC(C2)C1(C)C
mecamylamine
CNC1(C)C2CCC(C2)C1(C)C
mecamylamine
CN1CCCC1c1cccnc1
nicotine
CN1CCCC1c1cccnc1
nicotine
CNC1(C)C2CCC(C2)C1(C)C
mecamylamine
CN1CCCC1c1cccnc1
nicotine
CN1CCCC1c1cccnc1
Nicotine
CNC1(C)C2CCC(C2)C1(C)C
mecamylamine
CN1CCCC1c1cccnc1.CNC1(C)C2CCC(C2)C1(C)C
Nicotine Mecamylamine

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    Secado0.96 mg/cm2 nicotine, 0.40 mg/cm2 mecamylamine, 8.24 mg/cm2 adhesive for the second batch) and then dried at 30–40° C. for about 2 min.

Procedimiento

Nicotine and mecamylamine were added to a hexane solution of Dow Corning BIO-PSA amine compatible silicone pressure sensitive adhesive. Two batches were made: one contained approximately 10% nicotine and 6.4% mecamylamine based on the total dry weight of the adhesive and the two drugs; and a second contained approximately 10% nicotine and 4.2% mecamylamine, based on the total dry weight of the adhesive and the two drugs. The batches were separately coated onto a 3M Scotchpak 1109 polyester/polyoefin backing film at 9.6 mg/cm2 (0.96 mg/cm2 nicotine, 0.61 mg/cm2 mecamylamine, 8.03 mg/cm2 adhesive for the first batch; 0.96 mg/cm2 nicotine, 0.40 mg/cm2 mecamylamine, 8.24 mg/cm2 adhesive for the second batch) and then dried at 30–40° C. for about 2 min.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US06974588B1uspto-grants-2005_12