Reacción #571357

Ecuación de reacción

thiol

2,6-bis(1,1-dimethylethyl)-4-mercaptophenol

5-chloro-2-pentanone

triethylamine

→

title compound

5-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-2-pentanone

Disolventes

ethyl ether

Condiciones de reacción

Procedimiento

The thiol of Example 2 (5.0 g, 0.021M) was reacted with 5-chloro-2-pentanone (2.87 ml) and triethylamine (3.0 ml) in ethyl ether (50 ml) by the method of Example 8 to give the title compound, m.p. ca. 65°-67° C.

Fuente