Reacción #554121

ord-3fe6e74758784d1ea32908717caed672

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    Otroan oil obtained in 33 percent yield

Procedimiento

When an initial charge of 3.3 moles of phenylthiomethyl lithium per mole of olefin was employed, the product was 1-(2-methoxymethoxyphenyl)-1-(4-hydroxy-3-methoxy-2-methoxymethoxyphenyl)-cyclopropane, an oil obtained in 33 percent yield and identified by proton NMR spectroscopy.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US05158597uspto-grants-1992_10