Reacción #550223

Ecuación de reacción

crotonyl chloride

carnitine hydrochloride

ethyl ether

→

crotonoyl carnitine

Disolventes

trifluoroacetic acid

Condiciones de reacción

Tratamiento posterior

1. 1
   Otroa precipitate formed
2. 2
   FiltraciónThe precipitate was filtered off
3. 3
   Otrosuch in the subsequent reaction

Procedimiento

8 cc (0.08 moles) of crotonyl chloride were added to a solution of carnitine hydrochloride (8 grams; 0.04 moles) in trifluoroacetic acid. The reaction mixture was kept under stirring at 50° C. overnight. Subsequently, ethyl ether was added to the mixture and a precipitate formed. The precipitate was filtered off and used as such in the subsequent reaction.

Fuente