Reacción #53313

Ecuación de reacción

Triethylamine

Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-bromobutyrate

→

title compound

Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-3-butenoate

Disolventes

carbon tetrachloride

Condiciones de reacción

Tratamiento posterior

1. 1
   Filtraciónthe mixture can be filtered through a pad of silica gel few times
2. 2
   Concentraciónconcentrate

Procedimiento

Add Triethylamine to a solution of Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-bromobutyrate (Step E) in carbon tetrachloride. After stirring approximately for 4 hours, the mixture can be filtered through a pad of silica gel few times, and concentrate to give the title compound.

Fuente