Reacción #532292

ord-72ad7bca23034e38a90e9c015f91657d

Ecuación de reacción

Cc1cc(O)cc(C)c1Br
4-bromo-3,5-dimethylphenol
Cc1ccc(S(=O)(=O)OCCC(C)(C)O)cc1
3-hydroxy-3-methylbutyl 4-methylbenzene sulfonate
Cc1cc(OCCC(C)(C)O)cc(C)c1Br
compound
Rendimiento 101.9%
Cc1cc(OCCC(C)(C)O)cc(C)c1Br
4-(4-bromo-3,5-dimethylphenoxy)-2-methylbutan-2-ol
Rendimiento 101.9%

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

According to the method of (Example 10) <Step 2>, from 4-bromo-3,5-dimethylphenol (3.60 g) and 3-hydroxy-3-methylbutyl 4-methylbenzene sulfonate (5.09 g), the subject compound (5.24 g) was obtained as a colorless oil.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08476287B2uspto-grants-2013_07